By K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler

With contributions by means of quite a few specialists

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This is also demonstrated in the wide-angle X-ray diagram of such an unloaded sample where the (]-04) reflex of the elongated crystal modification is still observable alongside the corresponding reflex of the relaxed m-form. These data lead to the conclusion that in predominantly amorphous specimens the reversibility of the conformational transitions occurring during elongation is strongly hampered. For the polymer chains in the amorphous domains this can be understood in terms of the lack of a driving force such as the improved molecular packing efficiency of the relaxed crystal form 152).

Absorbances of the ~(CH2)and y(CH2)absorption bands as a function of strain: (A) 1459cm- l, (m) 916 cm -1 (or-form);(O) 1485 em -1, (A) 960 cm -t (t3-form) and maximum values, respectively, during elongation. Tadokoro et al. 15a)correlated the critical stress o* for the transition from the crumpled u-form to the extended [3-form with the stress at the maximum of the stress-optical coefficient of the [3-form and confirmed by variable temperature measurements that o* corresponds well to the plateau region in the stress-strain diagram.

The stress-strain diagram of such an experiment is shown in Fig. 41. The corresponding structural absorbance ratios AOl126/Ao1662 and the structural absorbance values A0166 / evaluated from the spectra taken simultaneously to the mechanical treatment are illustrated in Fig. 42 and reveal an interesting result. Thus, despite constant elongation the extent of crystallization further increases during the fast decay region of the stress-relaxation interval before it attains a maximum value. While an analogous behaviour can be observed for the dichroic function of the 1662 cm -~ absorption band a distinctly smaller relative effect was obtained when the dichroic function of the 1126 cm - 1 crystallinity band is plotted as a function of stress-relaxation time (Fig.

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